JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0002871
Submitter
The Noguchi Institute
Reaction ID
R-0000-002871
Regist Date
2012/06/21 20:04:59
REACTANT
MOLECULE ID
JCGG-COM0003768 (Reaction Tree)
Mol
2.8 micro mole
MOLECULE ID
JCGG-COM0000623
Reactant Type
Zn
Mol
4.3 mmol
MOLECULE ID
JCGG-COM0000491
Reactant Type
AcOH
Mol
4.9 mmol
PRODUCT
MOLECULE ID
JCGG-COM0003770 (Reaction Tree)
Yield
45%
REACTION DETAIL
Reaction Time
1 hour
Reaction Temp
NOT specified
Solvent
EtOAc (3.0mL)
Reaction Type
microwave irradiation (150W)
COMMENT
Keywords: Biantennary, N-glycans, LacNAc, LacdiNAc, SPPS
REFERENCE
Reference Id
REF-0000-000371
Issn
Electronic
Doi
10.1021/jo200149d
PubMed ID
21612260
Journal Name
The Journal of organic chemistry. (2011) 76 (13): 5229-39.
Article Title
Synthesis of biantennary complex-type nonasaccharyl asn building blocks for solid-phase glycopeptide synthesis.
Author
Masashi, Hagiwara; Mizuki, Dohi; Yuko, Nakahara; Keiko, Komatsu; Yuya, Asahina; Akiharu, Ueki; Hironobu, Hojo; Yoshiaki, Nakahara; Yukishige, Ito
Affiliation
Department of Applied Biochemistry, Institute of Glycoscience, Tokai University, 4-1-1 Kitakaname, Hiratsuka-shi, Kanagawa 259-1292, Japan.
Reference Id
REF-0000-000372
Source
J. Org. Chem. 2011, 76, 5229-5239
Doi
10.1021/jo200149d

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)