Reaction:JCGG-RAC0002794

JCGG ID		JCGG-RAC0002794
Submitter		The Noguchi Institute
Reaction ID		R-0000-002794
Regist Date		2012/06/21 19:49:56
REACTANT
MOLECULE ID		JCGG-COM0003656 (Reaction Tree)
	Mol	60 micro mole
MOLECULE ID		JCGG-COM0003657
	Reactant Type	KOOH (0.5 M, KOH/H2O2 = 1/2)
	Volume	0.36 mL
PRODUCT
MOLECULE ID		JCGG-COM0003658 (Reaction Tree)
	Product Type	intermediate 1
	Yield	98.3%
REACTION DETAIL
Reaction Time		overnight
Reaction Temp		4 degree C
Solvent		THF (1mL)
Comment		The reactants were mixed at 0 degree in Celsius before stirred at 4 degree.
COMMENT
Keywords: mannuronic acids, mannopyranosides, mannopyranosyl methyl uronate, all-cis-linked tetrasaccharide
REFERENCE
Reference Id		REF-0000-000367
	Issn	Electronic
	Doi	10.1021/jo201179p
	PubMed ID	21793528
	Journal Name	The Journal of organic chemistry. (2011) 76 (18): 7301-15.
	Article Title	Stereoselective synthesis of 2,3-diamino-2,3-dideoxy-β-D-mannopyranosyl uronates.
	Author	Marthe T C, Walvoort; Gert-Jan, Moggré; Gerrit, Lodder; Herman S, Overkleeft; Jeroen D C, Codée; Gijsbert A, van der Marel
	Affiliation	Leiden Institute of Chemistry, Leiden University, P.O. Box 9502, 2300 RA Leiden, The Netherlands.
Reference Id		REF-0000-000368
	Source	J. Org. Chem. 2011, 76, 7301-7315
	Doi	10.1021/jo201179p