JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0002782
Submitter
The Noguchi Institute
Reaction ID
R-0000-002782
Regist Date
2012/06/21 19:47:57
REACTANT
MOLECULE ID
JCGG-COM0003635 (Reaction Tree)
Mol
0.74 mmol
MOLECULE ID
JCGG-COM0000086
Reactant Type
Ac2O (solvent)
Volume
1.5 mL
MOLECULE ID
JCGG-COM0000979
Reactant Type
pyridine (solvent)
Volume
4.5 mL
PRODUCT
MOLECULE ID
JCGG-COM0003636 (Reaction Tree)
Yield
quantitative
REACTION DETAIL
Reaction Time
NOT specified
Reaction Temp
NOT specified
Solvent
Ac2O/pyridine
COMMENT
Keywords: mannuronic acids, mannopyranosides, mannopyranosyl methyl uronate, all-cis-linked tetrasaccharide
REFERENCE
Reference Id
REF-0000-000367
Issn
Electronic
Doi
10.1021/jo201179p
PubMed ID
21793528
Journal Name
The Journal of organic chemistry. (2011) 76 (18): 7301-15.
Article Title
Stereoselective synthesis of 2,3-diamino-2,3-dideoxy-β-D-mannopyranosyl uronates.
Author
Marthe T C, Walvoort; Gert-Jan, Moggré; Gerrit, Lodder; Herman S, Overkleeft; Jeroen D C, Codée; Gijsbert A, van der Marel
Affiliation
Leiden Institute of Chemistry, Leiden University, P.O. Box 9502, 2300 RA Leiden, The Netherlands.
Reference Id
REF-0000-000368
Source
J. Org. Chem. 2011, 76, 7301-7315
Doi
10.1021/jo201179p

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)