Reaction:JCGG-RAC0002717

JCGG ID		JCGG-RAC0002717
Submitter		The Noguchi Institute
Reaction ID		R-0000-002717
Regist Date		2012/06/21 19:42:16
REACTANT
MOLECULE ID		JCGG-COM0003545 (Reaction Tree)
	Mol	45 micro mole
MOLECULE ID		JCGG-COM0000979
	Reactant Type	pyridine (solvent)
	Volume	1.5 mL
MOLECULE ID		JCGG-COM0001024
	Reactant Type	AcSH (solvent)
	Volume	1.5 mL
PRODUCT
MOLECULE ID		JCGG-COM0003546 (Reaction Tree)
	Product Type	alpha
	Yield	40%(alpha/beta=1/1)
MOLECULE ID		JCGG-COM0003547 (Reaction Tree)
	Product Type	beta
	Yield	40%(alpha/beta=1/1)
REACTION DETAIL
Reaction Time		3 hours
Reaction Temp		room temp
Solvent		pyridine/AcSH
COMMENT
Keywords: Streptococcus pneumonia, SP1, zwitterionic polysaccharide, ZPs, cis-glycosidic bond
REFERENCE
Reference Id		REF-0000-000363
	Issn	Electronic
	Doi	10.1021/jo102363d
	PubMed ID	21341806
	Journal Name	The Journal of organic chemistry. (2011) 76 (6): 1692-706.
	Article Title	Galacturonic acid lactones in the synthesis of all trisaccharide repeating units of the zwitterionic polysaccharide Sp1.
	Author	Alphert E, Christina; Leendert J, van den Bos; Herman S, Overkleeft; Gijsbert A, van der Marel; Jeroen D C, Codée
	Affiliation	Leiden Institute of Chemistry, Leiden University, P.O. Box 9502, 2300 RA Leiden, The Netherlands.
Reference Id		REF-0000-000364
	Source	J. Org. Chem. 2011, 76, 1692-1706
	Doi	10.1021/jo102363d