JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0002379
Submitter
The Noguchi Institute
Reaction ID
R-0000-002379
Regist Date
2012/06/21 19:07:48
REACTANT
MOLECULE ID
JCGG-COM0003096 (Reaction Tree)
Mol
0.37 mmol
MOLECULE ID
JCGG-COM0001919
Reactant Type
Bu3SnH
Mol
0.44 mmol
MOLECULE ID
JCGG-COM0002547
Reactant Type
AIBN
Mol
0.03 mmol
PRODUCT
MOLECULE ID
JCGG-COM0003098 (Reaction Tree)
Yield
69%
REACTION DETAIL
Reaction Time
24 hours
Reaction Temp
66 degree C
Solvent
anhydrous THF
Comment
The reaction was conducted in a sealed tube.
COMMENT
Keywords: hemifluorinated surfactants, membrane proteins, perfluorohexane-based, AIBN, adsorption, micellization
REFERENCE
Reference Id
REF-0000-000335
Issn
Electronic
Doi
10.1021/jo102245c
PubMed ID
21384802
Journal Name
The Journal of organic chemistry. (2011) 76 (7): 2084-93.
Article Title
Propyl-ended hemifluorinated surfactants: synthesis and self-assembling properties.
Author
Maher, Abla; Grégory, Durand; Bernard, Pucci
Affiliation
Université d'Avignon et des Pays de Vaucluse, Faculté des Sciences, Equipe Chimie Bioorganique et Systèmes Amphiphiles, 33 rue Louis Pasteur, F-84000 Avignon, France.
Reference Id
REF-0000-000336
Source
J. Org. Chem. 2011, 76, 2084-2093
Doi
10.1021/jo102245c

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)