Reaction:JCGG-RAC0002239

JCGG ID		JCGG-RAC0002239
Submitter		The Noguchi Institute
Reaction ID		R-0000-002239
Regist Date		2012/06/21 18:53:26
REACTANT
MOLECULE ID		JCGG-COM0002910 (Reaction Tree)
	Mol	0.9 mmol
MOLECULE ID		JCGG-COM0001275
	Reactant Type	BH3*THF
	Mol	1.8 mmol
MOLECULE ID		JCGG-COM0000009
	Reactant Type	TMSOTf
	Mol	0.1 mmol
PRODUCT
MOLECULE ID		JCGG-COM0002915 (Reaction Tree)
	Yield	80%
REACTION DETAIL
Reaction Time		3 hours
Reaction Temp		room temp
Solvent		anhydrous CH2Cl2
COMMENT
Keywords: stereoselectivity, 2-azido-2-deoxygalactosyl donors, acetyl groups, temperature, computational methods
REFERENCE
Reference Id		REF-0000-000327
	Issn	Electronic
	Doi	10.1021/jo1025157
	PubMed ID	21574599
	Journal Name	The Journal of organic chemistry. (2011) 76 (13): 5207-18.
	Article Title	Study of the stereoselectivity of 2-azido-2-deoxygalactosyl donors: remote protecting group effects and temperature dependency.
	Author	Jane, Kalikanda; Zhitao, Li
	Affiliation	Department of Chemistry, Binghamton University, Binghamton, New York 13902, United States.
Reference Id		REF-0000-000328
	Source	J. Org. Chem. 2011, 76, 5207-5218
	Doi	10.1021/jo1025157