JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0002124
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-002124
Regist Date
 2012/06/21 18:36:36
REACTANT
MOLECULE ID
 JCGG-COM0002774 (Reaction Tree)
Skeleton
JCGG-STR015611
Mol
 0.07 mmol
PRODUCT
MOLECULE ID
 JCGG-COM0002775 (Reaction Tree)
Skeleton
JCGG-STR015611
Yield
 93%
REACTION DETAIL
Reaction Time
 15 minutes
Reaction Temp
 room temp
Solvent
 MeOH
Comment
 350 mg of Dowex-50WX8-200 ion-exchange resin was used.
COMMENT
Keywords: maradolipid, C. elegans, trehalose
ATTENTION: There is a numerical discrepancy between the scheme and the written method. (the reaction time)
REFERENCE
Reference Id
 REF-0000-000319
Issn
 Electronic
Doi
 10.1021/jo200979n
PubMed ID
 21739985
Journal Name
 The Journal of organic chemistry. (2011) 76 (16): 6866-70.
Article Title
 Synthesis of maradolipid.
Author
 Vikram A, Sarpe; Suvarn S, Kulkarni
Affiliation
 Department of Chemistry, Indian Institute of Technology Bombay, Mumbai 400076, India.
Reference Id
 REF-0000-000320
Source
 J. Org. Chem. 2011, 76, 6866-6870
Doi
 10.1021/jo200979n
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)