JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0002121
Submitter
The Noguchi Institute
Reaction ID
R-0000-002121
Regist Date
2012/06/21 18:36:11
REACTANT
MOLECULE ID
JCGG-COM0002768 (Reaction Tree)
Skeleton
JCGG-STR015611
Mol
3.31 mmol
MOLECULE ID
JCGG-COM0000842
Reactant Type
K2CO3
Mol
0.40 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002769 (Reaction Tree)
Skeleton
JCGG-STR015611
Yield
92%
REACTION DETAIL
Reaction Time
15 minutes, 1 hour
Reaction Temp
0 degree C, room temp
Solvent
MeOH/CH2Cl2 = 3/1
Comment
1) +all, 2) temperature change
COMMENT
Keywords: maradolipid, C. elegans, trehalose
There are multiple phases in this reaction.
REFERENCE
Reference Id
REF-0000-000319
Issn
Electronic
Doi
10.1021/jo200979n
PubMed ID
21739985
Journal Name
The Journal of organic chemistry. (2011) 76 (16): 6866-70.
Article Title
Synthesis of maradolipid.
Author
Vikram A, Sarpe; Suvarn S, Kulkarni
Affiliation
Department of Chemistry, Indian Institute of Technology Bombay, Mumbai 400076, India.
Reference Id
REF-0000-000320
Source
J. Org. Chem. 2011, 76, 6866-6870
Doi
10.1021/jo200979n

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)