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Glycan Syntheses |
JCGG ID |
JCGG-RAC0002082 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-002082
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Regist Date |
2012/06/21 18:32:35 | |||||||
| REACTANT | ||||||||
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Reactant Type |
alpha | |||||||
Mol |
0.42 mmol | |||||||
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||||||
Mol |
0.42 mmol | |||||||
|
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|||||||
Reactant Type |
TMSOTf | |||||||
Mol |
0.08 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
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Yield |
76% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
NOT specified | |||||||
Reaction Temp |
-78 degree C | |||||||
Solvent |
dry CH2Cl2 | |||||||
| COMMENT | ||||||||
| Keywords: glycosylthiols, bis-trimethyl-silyl sulfide, sterically hindered S-nucleophile | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000317 | |||||||
Issn |
Electronic | |||||||
Doi |
10.1021/jo200624e | |||||||
PubMed ID |
21800823 | |||||||
Journal Name |
The Journal of organic chemistry. (2011) 76 (18): 7539-45. | |||||||
Article Title |
Synthesis of glycosylthiols and reactivity studies. | |||||||
Author |
Ravindra T, Dere; Amit, Kumar; Vipin, Kumar; Xiangming, Zhu; Richard R, Schmidt | |||||||
Affiliation |
Fachbereich Chemie, Universita？t Konstanz, Fach 725, D-78457 Konstanz, Germany. | |||||||
Reference Id |
REF-0000-000318 | |||||||
Source |
J. Org. Chem. 2011, 76, 7539-7545 | |||||||
Doi |
10.1021/jo200624e | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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