JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001972
Submitter
The Noguchi Institute
Reaction ID
R-0000-001972
Regist Date
2012/06/21 18:19:45
REACTANT
MOLECULE ID
JCGG-COM0002467 (Reaction Tree)
MOLECULE ID
JCGG-COM0000531
Reactant Type
H2O
MOLECULE ID
JCGG-COM0000842
Reactant Type
K2CO3
MOLECULE ID
JCGG-COM0002573
Reactant Type
TfN3
PRODUCT
MOLECULE ID
JCGG-COM0002574 (Reaction Tree)
Product Type
intermediate
Yield
NOT specified
REACTION DETAIL
Reaction Time
NOT specified
Reaction Temp
NOT specified
Solvent
CH2Cl2/MeOH
Comment
Very few were described regarding this reaction.
CuSO4 was included in the solvent.
COMMENT
Keywords: synthesis, 2-deoxy-2-acetamido-glycopyranosides, 2-azido, A. Vasella, trifluoromethanesulfonyl azide, TfN3
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000307
Source
Helv. Chim. Acta 74, 2073 (1991)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)