JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001947
Submitter
The Noguchi Institute
Reaction ID
R-0000-001947
Regist Date
2012/06/21 18:16:54
REACTANT
MOLECULE ID
JCGG-COM0001983 (Reaction Tree)
Skeleton
JCGG-STR032525
MOLECULE ID
JCGG-COM0002534 (Reaction Tree)
MOLECULE ID
JCGG-COM0002535
Reactant Type
BSP
MOLECULE ID
JCGG-COM0000761
Reactant Type
Tf2O
MOLECULE ID
JCGG-COM0002536
Reactant Type
TTBP
PRODUCT
MOLECULE ID
JCGG-COM0002537 (Reaction Tree)
Yield
85%
REACTION DETAIL
Reaction Time
NOT specified
Reaction Temp
-60 degree C
Solvent
CH2Cl2
Comment
Very few were described regarding this reaction.
COMMENT
Keywords: synthesis, thioglycosides, BSP, Tf2O, TTBP
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000300
Source
J. Am. Chem. Soc. 123, 9015 (1991)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)