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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001924 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001924
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Regist Date |
2012/06/21 18:15:01 | |||||||
| REACTANT | ||||||||
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Reactant Type |
donor | |||||||
Mol |
32 mmol | |||||||
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Reactant Type |
acceptor | |||||||
Mol |
20 mmol | |||||||
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Reactant Type |
BF3*OEt2 | |||||||
Mol |
32.5 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
84% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
30 minutes | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
dry CH2Cl2 | |||||||
Comment |
The reactants were mixed at 0 degree in Celsius before stirred at room temperature. | |||||||
| COMMENT | ||||||||
| Keywords: synthesis, trichloroacetimidate method, BF3*OEt2 | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000253 | |||||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | |||||||
Reference Id |
REF-0000-000254 | |||||||
Source |
ISBN 978-3-527-31528-4 | |||||||
Reference Id |
REF-0000-000294 | |||||||
Source |
Liebigs Ann. Chem. 1099 (1989) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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