JCGG ID |
JCGG-RAC0001922 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001922 | |||||||
Regist Date |
2012/06/21 18:14:52 | |||||||
REACTANT | ||||||||
|
|
|||||||
Mol |
0.249 mmol | |||||||
|
|
|||||||
Reactant Type |
DBU | |||||||
Mol |
0.07 mmol | |||||||
|
|
|||||||
Reactant Type |
Cl3CCN | |||||||
Mol |
3 mmol | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Yield |
98% | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
10 minutes | |||||||
Reaction Temp |
-5 degree C | |||||||
Solvent |
dry Cl(CH2)2Cl | |||||||
COMMENT | ||||||||
Keywords: synthesis, trichloroacetimidate method, DBU | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000253 | |||||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | |||||||
Reference Id |
REF-0000-000254 | |||||||
Source |
ISBN 978-3-527-31528-4 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |