JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001922
Submitter
The Noguchi Institute
Reaction ID
R-0000-001922
Regist Date
2012/06/21 18:14:52
REACTANT
MOLECULE ID
JCGG-COM0002193 (Reaction Tree)
Mol
0.249 mmol
MOLECULE ID
JCGG-COM0000522
Reactant Type
DBU
Mol
0.07 mmol
MOLECULE ID
JCGG-COM0000521
Reactant Type
Cl3CCN
Mol
3 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002194 (Reaction Tree)
Skeleton
JCGG-STR032527
Yield
98%
REACTION DETAIL
Reaction Time
10 minutes
Reaction Temp
-5 degree C
Solvent
dry Cl(CH2)2Cl
COMMENT
Keywords: synthesis, trichloroacetimidate method, DBU
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4

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