JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001921
Submitter
The Noguchi Institute
Reaction ID
R-0000-001921
Regist Date
2012/06/21 18:14:50
REACTANT
MOLECULE ID
JCGG-COM0002191 (Reaction Tree)
Mol
8.61 mmol
MOLECULE ID
JCGG-COM0000842
Reactant Type
K2CO3
Weight
2 g
MOLECULE ID
JCGG-COM0000521
Reactant Type
Cl3CCN
Mol
24.8 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002192 (Reaction Tree)
Skeleton
JCGG-STR031569
Yield
54%
REACTION DETAIL
Reaction Time
2 hours
Reaction Temp
room temp
Solvent
dry CH2Cl2
COMMENT
Keywords: synthesis, trichloroacetimidate method, potassium carbonate
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4

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