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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001920 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001920
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Regist Date |
2012/06/21 18:14:47 | |||||||
| REACTANT | ||||||||
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Mol |
22.2 mmol | |||||||
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Reactant Type |
NaH | |||||||
Mol |
2.08 + 29.2 mmol | |||||||
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Reactant Type |
Cl3CCN | |||||||
Mol |
99 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
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Yield |
96% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
15 minutes + 2 hours | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
dry CH2Cl2 | |||||||
Comment |
The second addition of NaH was performed 15 minutes after the start of the reaction. | |||||||
| COMMENT | ||||||||
| Keywords: synthesis, trichloroacetimidate method, NaH | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000253 | |||||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | |||||||
Reference Id |
REF-0000-000254 | |||||||
Source |
ISBN 978-3-527-31528-4 | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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