|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0001901 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001901
|
||||
Regist Date |
2012/06/21 18:13:19 | ||||
| REACTANT | |||||
|
|
|
||||
Reactant Type |
intermediate 1 | ||||
|
|
|
||||
Reactant Type |
NaCNBH3 | ||||
|
|
|
||||
Reactant Type |
TMSCl | ||||
| PRODUCT | |||||
MOLECULE ID |
|
|
|||
Product Type |
intermediate 2 | ||||
Yield |
56% to 85% | ||||
| REACTION DETAIL | |||||
Reaction Time |
12 hours | ||||
Reaction Temp |
0 to 20 degree C | ||||
Solvent |
MeCN | ||||
Comment |
Very few were described regarding this reaction. | ||||
| COMMENT | |||||
| Keywords: synthesis, carbohydrate scaffolds, orthogonality | |||||
| The reaction is the 3rd part of the sequence. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000253 | ||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | ||||
Reference Id |
REF-0000-000254 | ||||
Source |
ISBN 978-3-527-31528-4 | ||||
Reference Id |
REF-0000-000288 | ||||
Source |
Angew. Chem. Int. Ed. 43, 1104 (2004) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|