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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001897 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001897
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Regist Date |
2012/06/21 18:13:00 | ||||
| REACTANT | |||||
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Reactant Type |
methyl mercaptopropionate | ||||
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Reactant Type |
BF3*OEt2 | ||||
| PRODUCT | |||||
MOLECULE ID |
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Product Type |
intermediate 1 | ||||
Yield |
30% to 55%(at least) | ||||
| REACTION DETAIL | |||||
Reaction Time |
12 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
CH2Cl2 | ||||
Comment |
Very few were described regarding this reaction. | ||||
| COMMENT | |||||
| Keywords: synthesis, carbohydrate scaffolds, orthogonality | |||||
| The reaction is the 2nd part of the sequence. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000253 | ||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | ||||
Reference Id |
REF-0000-000254 | ||||
Source |
ISBN 978-3-527-31528-4 | ||||
Reference Id |
REF-0000-000288 | ||||
Source |
Angew. Chem. Int. Ed. 43, 1104 (2004) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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