JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001896
Submitter
The Noguchi Institute
Reaction ID
R-0000-001896
Regist Date
2012/06/21 18:12:53
REACTANT
MOLECULE ID
JCGG-COM0002489 (Reaction Tree)
Reactant Type
intermediate
MOLECULE ID
JCGG-COM0000086
Reactant Type
Ac2O
MOLECULE ID
JCGG-COM0000979
Reactant Type
pyridine (solvent)
PRODUCT
MOLECULE ID
JCGG-COM0002490 (Reaction Tree)
Yield
73%
REACTION DETAIL
Reaction Time
12 hours
Reaction Temp
room temp
Solvent
pyridine (possibly with dioxane)
Comment
Very few were described regarding this reaction.
COMMENT
Keywords: synthesis, carbohydrate scaffolds, orthogonality
The reaction is the 1st part of the sequence.
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000288
Source
Angew. Chem. Int. Ed. 43, 1104 (2004)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)