JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0001886
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-001886
Regist Date
 2012/06/21 18:12:00
REACTANT
MOLECULE ID
 JCGG-COM0002467 (Reaction Tree)
MOLECULE ID
 JCGG-COM0002474
MOLECULE ID
 JCGG-COM0000086
Reactant Type
 Ac2O
MOLECULE ID
 JCGG-COM0000979
Reactant Type
 pyridine
PRODUCT
MOLECULE ID
 JCGG-COM0002473 (Reaction Tree)
Yield
 NOT specified
REACTION DETAIL
Reaction Time
 NOT specified, NOT specified
Reaction Temp
 NOT specified, NOT specified
Solvent
 EtOH, EtOH
Comment
 1) +all except Ac2O and pyridine 2) +Ac2O, pyridine
Very few were described regarding this reaction.
The pH of the solution was kept between 9 and 10. (first step)
COMMENT
Keywords: synthesis, N-protection, amino sugars, dithiasuccinoyl, NDts
The reaction is the 1st part of the sequence.
There are multiple steps in this reaction.
REFERENCE
Reference Id
 REF-0000-000253
Source
 Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
 REF-0000-000254
Source
 ISBN 978-3-527-31528-4
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)