JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001881
Submitter
The Noguchi Institute
Reaction ID
R-0000-001881
Regist Date
2012/06/21 18:11:30
REACTANT
MOLECULE ID
JCGG-COM0002465 (Reaction Tree)
Skeleton
JCGG-STR032134
Reactant Type
intermediate 2
MOLECULE ID
JCGG-COM0000491
Reactant Type
AcOH
Volume
15 mL
PRODUCT
MOLECULE ID
JCGG-COM0002466 (Reaction Tree)
Skeleton
JCGG-STR032134
Yield
70%(at least)
REACTION DETAIL
Reaction Time
NOT specified
Reaction Temp
NOT specified
Solvent
dry CH2Cl2
COMMENT
Keywords: synthesis, orthoesters, 2,4-di-O-benzoyl-6-deoxy-alpha-L-galactopyranoside, triethyl orthobenzoate
All the synthetic sequence took place in the same reaction vessel.
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000284
Source
Liebigs Ann. Chem. 1237 (1990)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)