JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001853
Submitter
The Noguchi Institute
Reaction ID
R-0000-001853
Regist Date
2012/06/21 18:09:03
REACTANT
MOLECULE ID
JCGG-COM0002401 (Reaction Tree)
Reactant Type
maltose
Weight
40 g
MOLECULE ID
JCGG-COM0000375
Reactant Type
Ph-CH(OMe)2
Volume
18 mL
MOLECULE ID
JCGG-COM0000498
Reactant Type
p-TsOH
Weight
50 mg
PRODUCT
MOLECULE ID
JCGG-COM0002428 (Reaction Tree)
Yield
43%
REACTION DETAIL
Reaction Time
6 hours
Reaction Temp
60 to 70 degree C
Solvent
dry DMF
Comment
DMF (solvent) was replenished occasionally.
COMMENT
Keywords: synthesis, 4',6'-O-benzylidene-maltose
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000272
Source
Carbohydr. Res. 268, 93 (1995)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)