JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001852
Submitter
The Noguchi Institute
Reaction ID
R-0000-001852
Regist Date
2012/06/21 18:08:59
REACTANT
MOLECULE ID
JCGG-COM0002414 (Reaction Tree)
Skeleton
JCGG-STR032525
Weight
9.7 g
MOLECULE ID
JCGG-COM0000375
Reactant Type
Ph-CH(OMe)2
Weight
7.6 g
MOLECULE ID
JCGG-COM0000498
Reactant Type
p-TsOH
Weight
25 mg
PRODUCT
MOLECULE ID
JCGG-COM0001971 (Reaction Tree)
Skeleton
JCGG-STR032525
Yield
82%
REACTION DETAIL
Reaction Time
1 hour
Reaction Temp
60 degree C
Solvent
dry DMF
COMMENT
Keywords: synthesis, methyl 4,6-O-benzylidene-alpha-D-glucopyranoside
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000271
Source
Carbohydr. Res. 21, 473 (1972)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)