JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001851
Submitter
The Noguchi Institute
Reaction ID
R-0000-001851
Regist Date
2012/06/21 18:08:57
REACTANT
MOLECULE ID
JCGG-COM0001648 (Reaction Tree)
Reactant Type
anhydrous glucose
Weight
10 g
MOLECULE ID
JCGG-COM0000754
Reactant Type
ZnCl2
Weight
40 g
MOLECULE ID
JCGG-COM0000710
Reactant Type
Ph-CHO (solvent)
Volume
200 mL
PRODUCT
MOLECULE ID
JCGG-COM0002427 (Reaction Tree)
Yield
50.4%(approximately; 7.5 g)
REACTION DETAIL
Reaction Time
4 hours
Reaction Temp
room temp
Solvent
pure Ph-CHO
COMMENT
Keywords: synthesis, 4,6-O-benzylidene-D-glucopyranose
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000270
Source
Meth. Carbohydr. Chem. 1, 107 (1962)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)