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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001849 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001849
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Regist Date |
2012/06/21 18:08:48 | ||||
| REACTANT | |||||
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Reactant Type |
D-arabinopyranose | ||||
Mol |
66.6 mmol (pyranose + furanose) | ||||
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Reactant Type |
D-arabinofuranose | ||||
Mol |
66.6 mmol (pyranose + furanose) | ||||
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Reactant Type |
TBDMSCl | ||||
Mol |
73 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
50%(at least) | ||||
| REACTION DETAIL | |||||
Reaction Time |
3.5 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
dry pyridine | ||||
| COMMENT | |||||
| Keywords: synthesis, TBDMS, 1,2,3-tri-O-acetyl-5-O-t-butyldimethylsilyl-D-arabinofuranose | |||||
| The reaction is the 1st part of the sequence. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000253 | ||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | ||||
Reference Id |
REF-0000-000254 | ||||
Source |
ISBN 978-3-527-31528-4 | ||||
Reference Id |
REF-0000-000269 | ||||
Source |
Th. K. Lindhorst, J. Thiem, unpublished | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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