JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001842
Submitter
The Noguchi Institute
Reaction ID
R-0000-001842
Regist Date
2012/06/21 18:08:14
REACTANT
MOLECULE ID
JCGG-COM0002414 (Reaction Tree)
Skeleton
JCGG-STR032525
Mol
25.7 mmol
MOLECULE ID
JCGG-COM0000830
Reactant Type
DBTO
Mol
56.6 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002415 (Reaction Tree)
Skeleton
JCGG-STR032525
Product Type
stannane
Yield
82%(at least)
REACTION DETAIL
Reaction Time
1 hour
Reaction Temp
70 degree C
Solvent
dry MeOH
COMMENT
Keywords: synthesis, methyl 2,6-di-O-benzyl-alpha-D-glucopyranoside
The reaction is the 1st part of the sequence.
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000267
Source
Tetrahedron Lett. 11, 3503 (1976)

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