JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001840
Submitter
The Noguchi Institute
Reaction ID
R-0000-001840
Regist Date
2012/06/21 18:07:59
REACTANT
MOLECULE ID
JCGG-COM0002408 (Reaction Tree)
Skeleton
JCGG-STR031569
Reactant Type
glucopyranoside
Mol
0.025 mmol
MOLECULE ID
JCGG-COM0001026
Reactant Type
Pd-C (10%)
Weight
0.1 g
MOLECULE ID
JCGG-COM0000414
Reactant Type
H2 (gas)
MOLECULE ID
JCGG-COM0002409
Reactant Type
Boc2O
Mol
3.75 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002410 (Reaction Tree)
Skeleton
JCGG-STR031569
Yield
90%
REACTION DETAIL
Reaction Time
6 hours
Reaction Temp
room temp
Solvent
EtOAc
COMMENT
Keywords: synthesis, Boc anhydride, 2,3,4,6-tetra-O-acetyl-beta-D-glucopyranoside
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000265
Source
Eur. J. Org. Chem. 2035 (2000)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)