JCGG ID |
JCGG-RAC0001834 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001834 | |||||||
Regist Date |
2012/06/21 18:07:15 | |||||||
REACTANT | ||||||||
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|
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Reactant Type |
L-fucose | |||||||
Weight |
1 g | |||||||
|
|
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Reactant Type |
BzCl | |||||||
Volume |
2.3 mL | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
|
|
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Yield |
65% | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
15 minutes | |||||||
Reaction Temp |
-40 degree C | |||||||
Solvent |
pyridine/CH2Cl2 | |||||||
Comment |
BzCl was added dropwise. | |||||||
COMMENT | ||||||||
Keywords: synthesis, regioselective acylation, L-fucose | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000253 | |||||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | |||||||
Reference Id |
REF-0000-000254 | |||||||
Source |
ISBN 978-3-527-31528-4 | |||||||
Reference Id |
REF-0000-000261 | |||||||
Source |
Carbohydr. Res. 209, 119 (1991) |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |