JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001834
Submitter
The Noguchi Institute
Reaction ID
R-0000-001834
Regist Date
2012/06/21 18:07:15
REACTANT
MOLECULE ID
JCGG-COM0002384 (Reaction Tree)
Reactant Type
L-fucose
Weight
1 g
MOLECULE ID
JCGG-COM0000392
Reactant Type
BzCl
Volume
2.3 mL
PRODUCT
MOLECULE ID
JCGG-COM0002396 (Reaction Tree)
Skeleton
JCGG-STR032134
Yield
65%
REACTION DETAIL
Reaction Time
15 minutes
Reaction Temp
-40 degree C
Solvent
pyridine/CH2Cl2
Comment
BzCl was added dropwise.
COMMENT
Keywords: synthesis, regioselective acylation, L-fucose
REFERENCE
Reference Id
REF-0000-000253
Source
Essentials of Carbohydrate Chemistry and Biochemistry
Reference Id
REF-0000-000254
Source
ISBN 978-3-527-31528-4
Reference Id
REF-0000-000261
Source
Carbohydr. Res. 209, 119 (1991)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)