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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001830 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001830
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Regist Date |
2012/06/21 18:06:55 | |||||||
| REACTANT | ||||||||
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Reactant Type |
D-glucose | |||||||
Mol |
0.3 mmol | |||||||
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Reactant Type |
NaOAc | |||||||
Mol |
0.3 mmol | |||||||
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Reactant Type |
Ac2O (solvent) | |||||||
Mol |
3.2 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
50% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
30 minutes, 2 hours | |||||||
Reaction Temp |
reflux, crushed ice | |||||||
Solvent |
Ac2O, Ac2O | |||||||
Comment |
1) +all, 2) temperature change | |||||||
| COMMENT | ||||||||
| Keywords: synthesis, penta-O-acetyl-beta-D-glucopyranose | ||||||||
| There are multiple steps in this reaction. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000253 | |||||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | |||||||
Reference Id |
REF-0000-000254 | |||||||
Source |
ISBN 978-3-527-31528-4 | |||||||
Reference Id |
REF-0000-000259 | |||||||
Source |
Meth. Carbohydr. Chem. 2, 211 (1963) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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