JCGG ID |
JCGG-RAC0001824 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001824 | |||||||
Regist Date |
2012/06/21 18:06:31 | |||||||
REACTANT | ||||||||
|
|
|||||||
Reactant Type |
L-fucose | |||||||
Mol |
60.9 mmol | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Yield |
84% | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
18 hours | |||||||
Reaction Temp |
reflux | |||||||
Solvent |
dry MeOH | |||||||
Comment |
10 g of strongly acidic ion exchange resin was included in the solvent. | |||||||
COMMENT | ||||||||
Keywords: synthesis, methyl alpha-L-fucoside, Fischer glycosylation | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000253 | |||||||
Source |
Essentials of Carbohydrate Chemistry and Biochemistry | |||||||
Reference Id |
REF-0000-000254 | |||||||
Source |
ISBN 978-3-527-31528-4 | |||||||
Reference Id |
REF-0000-000255 | |||||||
Source |
J. Org. Chem. 37, 2141 (1972) |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |