JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001823
Submitter
The Noguchi Institute
Reaction ID
R-0000-001823
Regist Date
2012/06/21 18:06:26
REACTANT
MOLECULE ID
JCGG-COM0002382 (Reaction Tree)
Mol
0.17 mmol
MOLECULE ID
JCGG-COM0002342 (Reaction Tree)
Mol
0.42 mmol
MOLECULE ID
JCGG-COM0000576
Reactant Type
DMTST
Mol
0.76 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002383 (Reaction Tree)
Yield
85%
REACTION DETAIL
Reaction Time
2 days
Reaction Temp
0 degree C
Solvent
CH2Cl2
Comment
58, 34, and MS 4A were mixed and stirred for 5 hours at room temperature before the reaction.
MS 4A was included in the solvent.
COMMENT
Keywords: synthesis, sialyl glycosides, ganglioside GQ1balpha oligosaccharide
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000252
Source
J. Carbohydr. Chem. 14:491 (1995)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)