JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001820
Submitter
The Noguchi Institute
Reaction ID
R-0000-001820
Regist Date
2012/06/21 18:05:05
REACTANT
MOLECULE ID
JCGG-COM0002377 (Reaction Tree)
Mol
0.25 mmol
MOLECULE ID
JCGG-COM0002343 (Reaction Tree)
Mol
0.38 mmol
MOLECULE ID
JCGG-COM0000576
Reactant Type
DMTST
Mol
0.76 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002378 (Reaction Tree)
Yield
52%
REACTION DETAIL
Reaction Time
2 days
Reaction Temp
0 degree C
Solvent
CH2Cl2
Comment
53, 35, and MS 4A were mixed and stirred for 5 hours at room temperature before the reaction.
MS 4A was included in the solvent.
COMMENT
Keywords: synthesis, sialyl glycosides, ganglioside GQ1b oligosaccharide
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000250
Source
Tetrahedron Asymm. 5:2493 (1994)
Reference Id
REF-0000-000251
Source
Carbohydr. Res. 260:C1 (1994)

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