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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001819 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001819
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Regist Date |
2012/06/21 18:04:23 | |||||||
| REACTANT | ||||||||
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Mol |
0.82 mmol | |||||||
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Mol |
1.6 mmol | |||||||
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Reactant Type |
NIS | |||||||
Mol |
3.3 mmol | |||||||
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Reactant Type |
TfOH | |||||||
Mol |
0.34 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
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Product Type |
alpha | |||||||
Yield |
50% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
24 hours | |||||||
Reaction Temp |
-25 degree C | |||||||
Solvent |
dry MeCN | |||||||
Comment |
51, 26, and MS 3A were mixed and stirred for 5 hours at room temperature before the reaction. | |||||||
| MS 3A was included in the solvent. | ||||||||
| COMMENT | ||||||||
| Keywords: synthesis, sialyl glycosides, ganglioside GD2 oligosaccharide | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000249 | |||||||
Source |
Carbohydr. Res. 252:283 (1994) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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