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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001818 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001818
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Regist Date |
2012/06/21 18:03:58 | |||||||
| REACTANT | ||||||||
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Mol |
1.05 mmol | |||||||
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Mol |
1.37 mmol | |||||||
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Reactant Type |
AgOTf | |||||||
Mol |
2.10 mmol | |||||||
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Reactant Type |
MSB | |||||||
Mol |
2.20 (1.10 + 1.10) mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Product Type |
beta | |||||||
Yield |
45% | |||||||
MOLECULE ID |
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Product Type |
beta | |||||||
Yield |
36% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
24 hours | |||||||
Reaction Temp |
-15 degree C | |||||||
Solvent |
dry CH2Cl2 | |||||||
Comment |
48, 34, and MS 4A were mixed and stirred for 8 hours at room temperature before the reaction. | |||||||
| MS 4A was included in the solvent. | ||||||||
| MSB was injected twice. (0 minutes, 30 minutes) | ||||||||
| COMMENT | ||||||||
| Keywords: synthesis, sialyl glycosides, sialyl lacto-, neolactotetraose | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000248 | |||||||
Source |
J. Carbohydr. Chem. 13:641 (1994) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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