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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001763 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001763
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Regist Date |
2012/06/21 17:53:28 | |||||||
| REACTANT | ||||||||
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Mol |
5.39 mmol | |||||||
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Mol |
4.15 mmol | |||||||
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Reactant Type |
NIS | |||||||
Mol |
5.39 mmol | |||||||
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Reactant Type |
TESOTf | |||||||
Mol |
0.530 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
78% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
5 + 10 minutes | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
CH2Cl2 | |||||||
Comment |
TESOTf was added 5 minutes after the initiation of the reaction. | |||||||
| COMMENT | ||||||||
| Keywords: oligosaccharide synthesis, n-pentenyl glycosides, Coupling, 1,2-Orthoesters, NIS/Et3SiOTf | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000236 | |||||||
Source |
J. Am. Chem. Soc. 117:1546 (1995) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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