JCGG ID |
JCGG-RAC0001761 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001761 | |||||||
Regist Date |
2012/06/21 17:53:12 | |||||||
REACTANT | ||||||||
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Mol |
13.5 mmol | |||||||
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Reactant Type |
Br2 (2.5 M in CH2Cl2) | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
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Yield |
NOT specified | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
until a faint yellow color persisted | |||||||
Reaction Temp |
0 degree C | |||||||
Solvent |
dry CH2Cl2 | |||||||
COMMENT | ||||||||
Keywords: oligosaccharide synthesis, n-pentenyl glycosides, 1,2-Orthoesters, Glycosyl Bromides, Coupling, Koenigs-Knorr Procedure | ||||||||
The reaction is the 1st part of the sequence. | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000236 | |||||||
Source |
J. Am. Chem. Soc. 117:1546 (1995) |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |