JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001759
Submitter
The Noguchi Institute
Reaction ID
R-0000-001759
Regist Date
2012/06/21 17:53:03
REACTANT
MOLECULE ID
JCGG-COM0002308 (Reaction Tree)
Skeleton
JCGG-STR024801
Mol
0.180 mmol
MOLECULE ID
JCGG-COM0002310
Reactant Type
SmI2 (0.1 M in THF)
Volume
4 mL
PRODUCT
MOLECULE ID
JCGG-COM0002309 (Reaction Tree)
Skeleton
JCGG-STR024801
Yield
NOT specified
REACTION DETAIL
Reaction Time
1 hour + (until the blue color persisted for at least 30 minutes)
Reaction Temp
room temp
Solvent
THF
COMMENT
Keywords: oligosaccharide synthesis, n-pentenyl glycosides, Reductive Debromination, Vicinal Dibromides
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000237
Source
J. Am. Chem. Soc. 59:4443 (1994)
Reference Id
REF-0000-000240
Source
J. Carbohydr. Chem. 15:65 (1996)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)