JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0001758
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-001758
Regist Date
 2012/06/21 17:52:59
REACTANT
MOLECULE ID
 JCGG-COM0002308 (Reaction Tree)
Skeleton
JCGG-STR024801
Mol
 0.180 mmol
MOLECULE ID
 JCGG-COM0000623
Reactant Type
 Zn
Mol
 0.918 mmol
MOLECULE ID
 JCGG-COM0000412
Reactant Type
 TBAI
Mol
 0.181 mmol
PRODUCT
MOLECULE ID
 JCGG-COM0002309 (Reaction Tree)
Skeleton
JCGG-STR024801
Yield
 95%
REACTION DETAIL
Reaction Time
 18 hours
Reaction Temp
 NOT specified
Solvent
 EtOAc/EtOH = 3mL/20mL
Comment
 sonication
COMMENT
Keywords: oligosaccharide synthesis, n-pentenyl glycosides, Reductive Debromination, Vicinal Dibromides
REFERENCE
Reference Id
 REF-0000-000196
Source
 PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
 REF-0000-000197
Source
 ISBN 0-8247-9802-3
Reference Id
 REF-0000-000237
Source
 J. Am. Chem. Soc. 59:4443 (1994)
Reference Id
 REF-0000-000240
Source
 J. Carbohydr. Chem. 15:65 (1996)
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)