|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0001757 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001757
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Regist Date |
2012/06/21 17:52:44 | |||||||
| REACTANT | ||||||||
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Mol |
9.11 mmol | |||||||
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Reactant Type |
Et4NBr | |||||||
Mol |
4.55 mmol | |||||||
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Reactant Type |
Br2 | |||||||
Mol |
9.11 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
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Yield |
82% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
until the brown color persisted | |||||||
Reaction Temp |
0 degree C | |||||||
Solvent |
CH2Cl2 | |||||||
Comment |
Br2 was added dropwise. | |||||||
| COMMENT | ||||||||
| Keywords: oligosaccharide synthesis, n-pentenyl glycosides, NPGs, Vicinal Dibromides | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000234 | |||||||
Source |
Synlett, 927 (1992) | |||||||
Reference Id |
REF-0000-000237 | |||||||
Source |
J. Am. Chem. Soc. 59:4443 (1994) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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