JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001756
Submitter
The Noguchi Institute
Reaction ID
R-0000-001756
Regist Date
2012/06/21 17:52:37
REACTANT
MOLECULE ID
JCGG-COM0002303 (Reaction Tree)
Skeleton
JCGG-STR031569
Mol
1.25 mmol
MOLECULE ID
JCGG-COM0002304 (Reaction Tree)
Skeleton
JCGG-STR032525
Mol
1.03 mmol
MOLECULE ID
JCGG-COM0000736
Reactant Type
IDCP
Mol
1.65 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002305 (Reaction Tree)
Skeleton
JCGG-STR005065
Yield
63%
REACTION DETAIL
Reaction Time
10 hours
Reaction Temp
room temp
Solvent
dry Et2O/CH2Cl2 = 4/1
Comment
MS 4A was included in the solvent.
The reaction was conducted in dark condition.
COMMENT
Keywords: oligosaccharide synthesis, n-pentenyl glycosides, NPG Coupling, IDCP
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000239
Source
Carbohydr. Res. 216:323 (1991)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)