JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001755
Submitter
The Noguchi Institute
Reaction ID
R-0000-001755
Regist Date
2012/06/21 17:52:23
REACTANT
MOLECULE ID
JCGG-COM0002300 (Reaction Tree)
Mol
0.886 mmol
MOLECULE ID
JCGG-COM0002301 (Reaction Tree)
Mol
1.09 mmol
MOLECULE ID
JCGG-COM0000129
Reactant Type
NIS
Mol
1.07 mmol
MOLECULE ID
JCGG-COM0001218
Reactant Type
TESOTf
Mol
1.24 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002302 (Reaction Tree)
Yield
66%
REACTION DETAIL
Reaction Time
15 minutes
Reaction Temp
room temp
Solvent
CH2Cl2
COMMENT
Keywords: oligosaccharide synthesis, n-pentenyl glycosides, NPG Coupling, NIS-Stoichiometric Et3SiOTf
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000238
Source
J. Am. Chem. Soc. 117:1554 (1995)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)