|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0001753 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001753
|
|||||||
Regist Date |
2012/06/21 17:51:18 | |||||||
| REACTANT | ||||||||
|
|
|
|
||||||
Mol |
11.62 mmol (at least) | |||||||
|
|
|
|||||||
Reactant Type |
NaOMe | |||||||
Mol |
11.4 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Yield |
81%(at least) | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
2 hours | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
MeOH/CH2Cl2 = 7/1 | |||||||
| COMMENT | ||||||||
| Keywords: oligosaccharide synthesis, n-pentenyl glycosides, NPGs, Orthoester Rearrangement | ||||||||
| The reaction is the 5th part of the sequence. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000236 | |||||||
Source |
J. Am. Chem. Soc. 117:1546 (1995) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|
