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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001749 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001749
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Regist Date |
2012/06/21 17:51:01 | |||||||
| REACTANT | ||||||||
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Mol |
91.35 mmol (approximately) | |||||||
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Reactant Type |
4-penten-1-ol | |||||||
Mol |
0.137 mol | |||||||
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|||||||
Reactant Type |
2,6-lutidine | |||||||
Mol |
0.284 mol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
86% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
5 days | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
CH2Cl2 | |||||||
| COMMENT | ||||||||
| Keywords: oligosaccharide synthesis, n-pentenyl glycosides, NPGs, Orthoester Rearrangement | ||||||||
| The reaction is the 1st part of the sequence. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000236 | |||||||
Source |
J. Am. Chem. Soc. 117:1546 (1995) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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