JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001748
Submitter
The Noguchi Institute
Reaction ID
R-0000-001748
Regist Date
2012/06/21 17:50:53
REACTANT
MOLECULE ID
JCGG-COM0002288 (Reaction Tree)
Mol
8.45 mmol
MOLECULE ID
JCGG-COM0001013
Reactant Type
4-penten-1-ol
Mol
17.4 mmol
MOLECULE ID
JCGG-COM0000783
Reactant Type
SnCl4
Mol
8.5 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002289 (Reaction Tree)
Skeleton
JCGG-STR032527
Yield
80%
REACTION DETAIL
Reaction Time
30 minutes
Reaction Temp
room temp
Solvent
CH2Cl2
Comment
MS 4A was included in the solvent.
COMMENT
Keywords: oligosaccharide synthesis, n-pentenyl glycosides, NPGs, Glycosyl Acetates
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000234
Source
Synlett, 927 (1992)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)