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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001747 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001747
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Regist Date |
2012/06/21 17:50:45 | |||||||
| REACTANT | ||||||||
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Mol |
3.79 mmol | |||||||
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Reactant Type |
4-penten-1-ol | |||||||
Mol |
4.84 mmol | |||||||
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|||||||
Reactant Type |
AgOTf | |||||||
Mol |
4.67 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
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Yield |
68% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
10 minutes + 2 hours | |||||||
Reaction Temp |
-30 degree C | |||||||
Solvent |
CH2Cl2 | |||||||
Comment |
MS 4A was included in the solvent. | |||||||
| 60 was added through a syringe during 10 minutes. | ||||||||
| COMMENT | ||||||||
| Keywords: oligosaccharide synthesis, n-pentenyl glycosides, NPGs, Koenigs-Knorr Procedure | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000235 | |||||||
Source |
J. Org. Chem. 60:772 (1995) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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