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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001742 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001742
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Regist Date |
2012/06/21 17:49:52 | ||||
| REACTANT | |||||
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Mol |
0.057 mmol | ||||
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Reactant Type |
DAST | ||||
Mol |
0.08 mmol | ||||
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Reactant Type |
NBS | ||||
Mol |
0.08 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
83% | ||||
| REACTION DETAIL | |||||
Reaction Time |
1 hour | ||||
Reaction Temp |
room temp | ||||
Solvent |
CH2Cl2 | ||||
Comment |
The reactants were mixed at 0 degree in Celsius before stirred at room temperature. | ||||
| COMMENT | |||||
| Keywords: glycosyl fluorides, glycosyl sulfides, elfamycin | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000196 | ||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | ||||
Reference Id |
REF-0000-000197 | ||||
Source |
ISBN 0-8247-9802-3 | ||||
Reference Id |
REF-0000-000231 | ||||
Source |
J. Am. Chem. Soc. 107:1691 (1985) | ||||
Reference Id |
REF-0000-000232 | ||||
Source |
J. Am. Chem. Soc. 107:1695 (1985) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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