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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001741 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001741
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Regist Date |
2012/06/21 17:49:45 | |||||||
| REACTANT | ||||||||
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Mol |
0.15 mmol | |||||||
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Mol |
1.5 mmol | |||||||
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Reactant Type |
AgClO4 | |||||||
Mol |
0.30 mmol | |||||||
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Reactant Type |
SnCl2 | |||||||
Mol |
0.30 mmol | |||||||
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Reactant Type |
2,6-lutidine | |||||||
Volume |
17 micro L | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
80% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
10 minutes, 12 hours | |||||||
Reaction Temp |
0 degree C, room temp | |||||||
Solvent |
CH2Cl2, CH2Cl2 | |||||||
Comment |
1) 47+AgClO4, SnCl2, MS 4A, 2) +48, 2,6-lutidine | |||||||
| MS 4A was included in the solvent. | ||||||||
| COMMENT | ||||||||
| Keywords: glycosyl fluorides, glycosyl sulfides, globotriaosylceramide, Gb3 | ||||||||
| There are multiple steps in this reaction. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000230 | |||||||
Source |
Carbohydr. Res. 202:177 (1990) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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