JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001740
Submitter
The Noguchi Institute
Reaction ID
R-0000-001740
Regist Date
2012/06/21 17:49:33
REACTANT
MOLECULE ID
JCGG-COM0002071 (Reaction Tree)
Mol
0.453 mmol (at least)
MOLECULE ID
JCGG-COM0000086
Reactant Type
Ac2O
Volume
283 micro L
MOLECULE ID
JCGG-COM0000500
Reactant Type
DMAP
Weight
10 mg
MOLECULE ID
JCGG-COM0000979
Reactant Type
pyridine (solvent)
Volume
5 mL
PRODUCT
MOLECULE ID
JCGG-COM0002275 (Reaction Tree)
Yield
91%(at least)
REACTION DETAIL
Reaction Time
overnight
Reaction Temp
NOT specified
Solvent
pyridine
COMMENT
Keywords: glycosyl fluorides, glycosyl sulfides, globotriaosylceramide, Gb3
The reaction is the 3rd part of the sequence.
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000230
Source
Carbohydr. Res. 202:177 (1990)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)