|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0001737 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001737
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Regist Date |
2012/06/21 17:49:20 | |||||||
| REACTANT | ||||||||
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|||||||
Mol |
0.23 mmol | |||||||
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|
|
|
||||||
Mol |
0.70 mmol | |||||||
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|
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|||||||
Reactant Type |
AgOTf | |||||||
Mol |
0.70 mmol | |||||||
|
|
|
|||||||
Reactant Type |
Cp2HfCl2 | |||||||
Mol |
0.70 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
|
||||||
Yield |
58% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
1 hour | |||||||
Reaction Temp |
0 degree C | |||||||
Solvent |
CH2Cl2 | |||||||
Comment |
MS 4A was included in the solvent. | |||||||
| COMMENT | ||||||||
| Keywords: glycosyl fluorides, glycosyl sulfides, sulfated Lea tetrasaccharide | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000229 | |||||||
Source |
J. Am. Chem. Soc. 115:8843 (1990) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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