JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001734
Submitter
The Noguchi Institute
Reaction ID
R-0000-001734
Regist Date
2012/06/21 17:48:18
REACTANT
MOLECULE ID
JCGG-COM0002265 (Reaction Tree)
Skeleton
JCGG-STR028671
Mol
0.14 mmol
MOLECULE ID
JCGG-COM0000810
Reactant Type
DAST
Mol
0.27 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002266 (Reaction Tree)
Product Type
alpha
Yield
78%(alpha/beta=1/4)
MOLECULE ID
JCGG-COM0002267 (Reaction Tree)
Product Type
beta
Yield
78%(alpha/beta=1/4)
REACTION DETAIL
Reaction Time
15 minutes
Reaction Temp
-78 degree C
Solvent
CH2Cl2
COMMENT
Keywords: glycosyl fluorides, glycosyl sulfides, sialyl dimeric Lex
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000228
Source
J. Am. Chem. Soc. 114:3126 (1992)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)