JCGG ID |
JCGG-RAC0001731 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001731 | ||||
Regist Date |
2012/06/21 17:46:03 | ||||
REACTANT | |||||
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|
||||
Reactant Type |
(in 3.5 mL of Et2O) | ||||
Mol |
0.25 mmol | ||||
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|
||||
Reactant Type |
(in 3.5 mL of Et2O) | ||||
Mol |
0.25 mmol | ||||
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|
||||
Reactant Type |
AgClO4 | ||||
Mol |
0.46 mmol | ||||
|
|
||||
Reactant Type |
SnCl2 | ||||
Mol |
0.46 mmol | ||||
PRODUCT | |||||
MOLECULE ID |
|
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Yield |
66% | ||||
REACTION DETAIL | |||||
Reaction Time |
2 minutes + 2 hours, 10 hours | ||||
Reaction Temp |
-15 degree C, room temp | ||||
Solvent |
Et2O, Et2O | ||||
Comment |
1) +all, 2) temperature change | ||||
13 was added 2 minutes after the initiation of the reaction. | |||||
MS 4A was included in the solvent. | |||||
COMMENT | |||||
Keywords: glycosyl fluorides, glycosyl sulfides, hexasaccharide | |||||
There are multiple steps in this reaction. | |||||
ATTENTION: The reference is wrong. | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000196 | ||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | ||||
Reference Id |
REF-0000-000197 | ||||
Source |
ISBN 0-8247-9802-3 | ||||
Reference Id |
REF-0000-000226 | ||||
Source |
unknown |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |