Reaction:JCGG-RAC0001731

JCGG ID		JCGG-RAC0001731
Submitter		The Noguchi Institute
Reaction ID		R-0000-001731
Regist Date		2012/06/21 17:46:03
REACTANT
MOLECULE ID		JCGG-COM0002257 (Reaction Tree)
	Reactant Type	(in 3.5 mL of Et2O)
	Mol	0.25 mmol
MOLECULE ID		JCGG-COM0002256 (Reaction Tree)
	Reactant Type	(in 3.5 mL of Et2O)
	Mol	0.25 mmol
MOLECULE ID		JCGG-COM0000032
	Reactant Type	AgClO4
	Mol	0.46 mmol
MOLECULE ID		JCGG-COM0000813
	Reactant Type	SnCl2
	Mol	0.46 mmol
PRODUCT
MOLECULE ID		JCGG-COM0002258 (Reaction Tree)
	Yield	66%
REACTION DETAIL
Reaction Time		2 minutes + 2 hours, 10 hours
Reaction Temp		-15 degree C, room temp
Solvent		Et2O, Et2O
Comment		1) +all, 2) temperature change
		13 was added 2 minutes after the initiation of the reaction.
		MS 4A was included in the solvent.
COMMENT
Keywords: glycosyl fluorides, glycosyl sulfides, hexasaccharide
There are multiple steps in this reaction.
ATTENTION: The reference is wrong.
REFERENCE
Reference Id		REF-0000-000196
	Source	PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id		REF-0000-000197
	Source	ISBN 0-8247-9802-3
Reference Id		REF-0000-000226
	Source	unknown